1965
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- OverviewSep 16, 1966-Apr 14, 196730 episodesEpisodes30. The Cap and Gown Affair Apr 14, 1967
- THRUSH uses student demonstrators as a front for plot to kill Waverly.
- 29. The Five Daughters Affair Apr 7, 1967
- Solo and Illya travel from Japan to the polar icecap to stop THRUSH.
- 28. The Five Daughters Affair Mar 31, 1967
- Before he dies, a scientist learns how to extract gold from seawater.
- 27. The Apple a Day Affair Mar 24, 1967
- THRUSH plots to detonate a nuclear stockpile using explosive apples.
- 26. The When in Rome Affair Mar 17, 1967
- Solo drops a concealed formula into an American tourist's purse.
- 25. The Hot Number Affair Mar 10, 1967
- Innocents are endangered by searching agents.
- 24. The Matterhorn Affair Mar 3, 1967
- Solo and Illya search for the plans for a miniature atomic reactor.
- 23. The Pieces of Fate Affair Feb 24, 1967
- Sensitive THRUSH diaries are sought by Solo, Illya -- and THRUSH.
- 22. The Hula Doll Affair Feb 17, 1967
- Solo and Illya race against time to find THRUSH's New York quarters.
- 21. The It's All Greek to Me Affair Feb 3, 1967
- A Greek thief plans to sell a stolen U.N.C.L.E. code to THRUSH, unless Solo and Illya can stop him.
- 20. The Napoleon's Tomb Affair Jan 27, 1967
- As Solo and Illya guard a North African leader in Paris, THRUSH plots to rob Napoleon's tomb.
- 19. The Yo Ho Ho and a Bottle of Rum Affair Jan 20, 1967
- THRUSH uses a tidal-wave device for extortion.
- 18. The Deadly Smorgasbord Affair Jan 13, 1967
- Solo races for possession of a Swedish suspended-animation device.
- 17. The Suburbia Affair Jan 6, 1967
- Solo and Illya search for a missing Danish scientist who has discovered the secret of antimatter.
- 16. The Take Me to Your Leader Affair Dec 30, 1966
- An astronomer's daughter helps solve a UFO hoax.
- 15. The Jingle Bells Affair Dec 23, 1966
- A European leader becomes an assassination target at Christmastime.
- 14. The My Friend the Gorilla Affair Dec 16, 1966
- The agents must stop a mad scientist's experiments on African natives.
- 13. The Abominable Snowman Affair Dec 9, 1966
- A prime minister schemes to seize power in a tiny Himalayan kingdom.
- 12. The Concrete Overcoat Affair Dec 2, 1966
- Solo must save Illya and end THRUSH's plans to divert the Gulf Stream.
- 11. The Concrete Overcoat Affair Nov 25, 1966
- Wine merchant (Jack Palance) is somehow connected to a Nazi scientist.
- 10. The Come With Me to the Casbah Affair Nov 21, 1966
- A volume of 14th-century poetry holds the key to THRUSH codes.
- 9. The Off-Broadway Affair Nov 18, 1966
- U.N.C.L.E. communications break down after an actor who tried calling in dies.
- 8. The Candidate's Wife Affair Nov 4, 1966
- A THRUSH agent poses as a presidential candidate's wife (Diana Hyland in a dual role).
- 7. The Thor Affair Oct 28, 1966
- A munitions manufacturer plans to blow up a peace conference.
- 6. The Pop Art Affair Oct 21, 1966
- A dying defector reveals THRUSH's plan to defeat America with gas that causes fatal hiccups.
- 5. The Monks of St. Thomas Affair Oct 14, 1966
- THRUSH hides a laser gun in an Alpine monastery to threaten the capitals of Europe.
- 4. The Super-Colossal Affair Oct 7, 1966
- A crime czar plots to control a movie studio and bomb Las Vegas.
- 3. The Galatea Affair Sep 30, 1966
- A THRUSH contact is replaced by an actress.
- 2. The Sort of Do-It-Yourself Dreadful Affair Sep 23, 1966
- New race of assassins are immune to bullets.
- 1. The Her Master's Voice Affair Sep 16, 1966
- Solo and Illya investigate a diabolical plot at a ritzy girls school.