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2. webbook.nist.gov › cgi › cbookN-Phenylcyclohexylamine - NIST Chemistry WebBook

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   Feb 6, 2010 · N-Phenylcyclohexylamine. Formula: C 12 H 17 N. Molecular weight: 175.2701. IUPAC Standard InChI: InChI=1S/C12H17N/c1-3-7-11 (8-4-1)13-12-9-5-2-6-10-12/h1,3-4,7-8,12-13H,2,5-6,9-10H2. Copy Sheet of paper on top of another sheet. IUPAC Standard InChIKey: TXTHKGMZDDTZFD-UHFFFAOYSA-N.

3. chem.libretexts.org › Bookshelves › Organic_Chemistry24.6: Synthesis of Amines - Chemistry LibreTexts

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   Alkylation is an efficient method for the synthesis of 3 o and 4 o amines. However, when 1 o and 2 o amines are alkylated a mixture of products is typically produced. When ammonia is reacted with an alkylhalide an monoalkylammonium salt is formed. RX + NH 3 → RNH 3+ + X -.

4. People also ask

   How are arylamines prepared?

   • Arylamines are typically prepared by the reduction of a nitro group on an aromatic ring. Several methods for reducing nitro groups to amines are known. These include catalytic hydrogenation (H 2 + platinum catalyst), and zinc, iron, or tin (II) chloride in dilute mineral acid. The procedures described above are sufficient for most cases.

   24.6: Synthesis of Amines - Chemistry LibreTexts

   chem.libretexts.org/Bookshelves/Organic_Chemistry/Organic_Chemistry_(Morsch_et_al.)/24:_Amines_and_Heterocycles/24.06:_Synthesis_of_Amines

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   How amines are synthesised?

   • Another common method for the synthesis of 1 o amines is called the Gabriel amine synthesis. This reaction starts with the deprotonation of phthalimide by a hydroxide base such as potassium hydroxide (KOH). The N-H hydrogen of an imide functional group is acidic because its conjugate base is resonance stabilized by two carbonyl groups.

   24.6: Synthesis of Amines - Chemistry LibreTexts

   chem.libretexts.org/Bookshelves/Organic_Chemistry/Organic_Chemistry_(Morsch_et_al.)/24:_Amines_and_Heterocycles/24.06:_Synthesis_of_Amines

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   How do you plan a synthesis using reductive amination?

   • Planning a Synthesis using a Reductive Amination If you are trying to develop a synthesis of an amine molecule, the key bond break is a C-N bond in the target molecule. There may be multiple C-N bonds present, so each should be broken separately to produce a possible set of starting materials.

   24.6: Synthesis of Amines - Chemistry LibreTexts

   chem.libretexts.org/Bookshelves/Organic_Chemistry/Organic_Chemistry_(Morsch_et_al.)/24:_Amines_and_Heterocycles/24.06:_Synthesis_of_Amines

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   Which pathway provides the simplest amine starting material?

   • Because the amine is commonly used in excess during a reductive animation, the pathway which provides the simplest amine starting material is preferred. The carbon from the broken C-N bond goes on to become a carbonyl starting material. The nitrogen gains a hydrogen to become the amine starting material.

   24.6: Synthesis of Amines - Chemistry LibreTexts

   chem.libretexts.org/Bookshelves/Organic_Chemistry/Organic_Chemistry_(Morsch_et_al.)/24:_Amines_and_Heterocycles/24.06:_Synthesis_of_Amines

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5. pubchem.ncbi.nlm.nih.gov › 1-phenylcyclohexylamine1-Phenylcyclohexylamine | C12H17N | CID 31862 - PubChem

   pubchem.ncbi.nlm.nih.gov › 1-phenylcyclohexylamine

   Oct 14, 2021 · USA.gov. 1-Phenylcyclohexylamine | C12H17N | CID 31862 - structure, chemical names, physical and chemical properties, classification, patents, literature, biological activities, safety/hazards/toxicity information, supplier lists, and more.

6. chemistry.mdma.ch › hiveboard › rhodiumUse of PCA (1-phenylcyclohexylamine) as a precursor

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   Synthesis of PCP from PCA via 1-phenylcyclohexanol (PCOH) The PCOH starting material can be purchased or prepared by reaction of phenyllithium or phenyl grignard with cyclohexanone. This alcohol is then be transformed into the amine by reaction with sodium azide (~90% yield) followed by reduction.

7. www.erowid.org › archive › rhodiumThe Synthesis of Phencyclidine and Other 1 ... - Erowid

   www.erowid.org › archive › rhodium

   thesis of 1-phenylcyclohexylamine. The compound prepared by the alternate route (method F) was identi- cal in all respects with the one obtained prepared from Method F aC6"I NCO - CxCeH5 "2 VI phenylcyclohexene. Recently, Cristol, et ul., re- ported the isolation of the amine as its benzoyl deriva- tive via a modified Ritter reaction.

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8. chem.libretexts.org › Courses › Sacramento_City10.10: An Introduction to Multiple Step Synthesis - Chemistry ...

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   Feb 13, 2019 · William Reusch, Professor Emeritus ( Michigan State U. ), Virtual Textbook of Organic Chemistry. 10.10: An Introduction to Multiple Step Synthesis. Integrating the different reactions from the first 10 chapters of this text into multiple step synthetic pathways is an important skill in mastering organic chemistry.

9. pubs.acs.org › doi › 101-Phenylcycloalkylamine derivatives. II. Synthesis and ...

   pubs.acs.org › doi › 10

   Synthesis of deuterium‐labelled drugs of abuse for use as internal standards in quantification by selected ion monitoring. I. Methamphetamine; 2,5‐dimethoxy‐4‐methylamphetamine (DOM); phencyclidine (PCP); and methaqualone. Journal of Labelled Compounds and Radiopharmaceuticals 1976, 12 (1) , 69-78.