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1-Phenylcyclohexylamine | C12H17N | CID 31862 - structure, chemical names, physical and chemical properties, classification, patents, literature, biological activities, safety/hazards/toxicity information, supplier lists, and more.
Alkylation is an efficient method for the synthesis of 3 o and 4 o amines. However, when 1 o and 2 o amines are alkylated a mixture of products is typically produced. When ammonia is reacted with an alkylhalide an monoalkylammonium salt is formed. RX + NH 3 → RNH 3+ + X -.
Reaction schemes with PCA intermediate. The next three routes use PCA (1-phenyl cyclohexylamine) as a precursor for either PCP or other analogs. PCA itself is an active compound, and has been under clinical study as a potential anesthetic agent. It is approximately one half as potent than PCP and appears to have similar actions.
thesis of 1-phenylcyclohexylamine. The compound prepared by the alternate route (method F) was identi- cal in all respects with the one obtained prepared from Method F aC6"I NCO - CxCeH5 "2 VI phenylcyclohexene. Recently, Cristol, et ul., re- ported the isolation of the amine as its benzoyl deriva- tive via a modified Ritter reaction.
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- 1959/09/22
- MONSANTO (J. FREEMAN)
- N-cyclohexylanilineN-cyclohexyl-N-phenylamine
- COBLENTZ NO. 08474
An expedient synthesis of high specific activity tritium labelled 4‐fluoro‐1‐[1‐(2‐thienyl)]cyclohexylpiperidine ([ 3 H]FTCP), a ligand for further characterization of the phencyclidine/NMDA receptor complex.
Allow the layers to separate in the funnel, and then run and discard the aqueous layer. Run the organic layer into a clean, dry conical flask and add three spatula loads of drying agent (e.g. anhydrous sodium sulfate, calcium chloride) to dry the organic liquid. When dry the organic liquid should appear clear.
