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Because N-methylbenzylamine has two C-N bonds there are two possible synthesis pathways. Pathway 1 is most likely preferred because it uses the simplest amine starting material, methyl amine. Exercise \(\PageIndex{1}\)
OCR, A Level, Chemistry A, Topic Exploration Pack, Reaction pathways Created Date: 20170207082346Z ...
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A synthetic pathway is the route taken to prepare a specific product. For IB examinations syntheses of up to four steps are required. A schematic diagram of all of the required reactions is shown below:
thesis of 1-phenylcyclohexylamine. The compound prepared by the alternate route (method F) was identi- cal in all respects with the one obtained prepared from Method F aC6"I NCO - CxCeH5 "2 VI phenylcyclohexene. Recently, Cristol, et ul., re- ported the isolation of the amine as its benzoyl deriva- tive via a modified Ritter reaction.
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Revision notes on 7.8.2 Multi-step Synthetic Routes for the CIE A Level Chemistry syllabus, written by the Chemistry experts at Save My Exams.
Feb 6, 2010 · N-Phenylcyclohexylamine. Formula: C 12 H 17 N. Molecular weight: 175.2701. IUPAC Standard InChI: InChI=1S/C12H17N/c1-3-7-11 (8-4-1)13-12-9-5-2-6-10-12/h1,3-4,7-8,12-13H,2,5-6,9-10H2. Copy Sheet of paper on top of another sheet. IUPAC Standard InChIKey: TXTHKGMZDDTZFD-UHFFFAOYSA-N.
Synthesis of PCP from PCA via 1-phenylcyclohexanol (PCOH) The PCOH starting material can be purchased or prepared by reaction of phenyllithium or phenyl grignard with cyclohexanone. This alcohol is then be transformed into the amine by reaction with sodium azide (~90% yield) followed by reduction.
